毛細管柱檢測聚碳酸酯材料中酚類化合物，液化石油氣，二甲醚，甲縮醛，乙縮醛，乙醇，室內空氣，焦爐煤氣，煉廠氣，天然氣，變壓器油，多氯聯苯，植物油，增塑劑，塑化劑，過氧化物

毛細管柱檢測聚碳酸酯材料中酚類化合物
毛細管柱檢測聚碳酸酯材料中酚類化合物 詳細信息：

名稱：毛細管柱
固定相：5%苯基-95%甲基聚硅氧烷
規格：30m*0.25mm*0.25um
型號：HH-5
應用：T/HZAS 19-2021 聚碳酸酯材料 酚類化合物的測定 氣相色譜-質譜法


浩瀚色譜（山東）應用技術開發有限公司建立了快速檢測聚碳酸酯塑料包裝材料中2-叔丁基苯酚、4-叔丁基苯酚及2,4-二叔丁基苯酚等酚類化合物的氣相色譜質譜聯用法。樣品經正己烷超聲萃取離心、濃縮后進行GC/MS測定,外標法定量。結果表明,2-叔丁基苯酚、4-叔丁基苯酚及2,4-二叔丁基苯酚均分別在0.1100 mg/L范圍內線性關系良好;定量限（以信噪比≥10計）為1 mg/kg;在4個加標水平下3種酚類化合物的加標回收率為82.23%92.31%,相對標準偏差為2.13%4.76%（n=6）。該方法具有優異的靈敏度和穩定性,滿足對聚碳酸酯塑料包裝材料中2-叔丁基苯酚、4-叔丁基苯酚及2,4-二叔丁基苯酚等酚類化合物的分析檢測和準確定量。 


毛細管柱檢測聚碳酸酯材料中酚類化合物   測試譜圖：



Detection of Phenolic Compounds in Polycarbonate by Capillary Column
Capillary Column Detection of Phenolic Compounds in Polycarbonate Materials Details:

Name: capillary column
Stationary Phase: 5% Phenyl-95% Methylpolysiloxane
Specifications: 30m*0.25mm*0.25um
Model: HH-5
Application: T/HZAS 19-2021 Polycarbonate Materials Determination of Phenolic Compounds Gas Chromatography-Mass Spectrometry


Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has established a gas-phase rapid detection method for phenolic compounds such as 2-tert-butylphenol, 4-tert-butylphenol and 2,4-di-tert-butylphenol in polycarbonate plastic packaging materials. Chromatography mass spectrometry. The samples were extracted by n-hexane ultrasonic extraction, centrifuged, concentrated, and then determined by GC/MS, and quantified by external standard method. The results showed that 2-tert-butylphenol, 4-tert-butylphenol and 2,4-di-tert-butylphenol had good linear relationships in the range of 0.1100 mg/L, respectively. The recovery rates of the three phenolic compounds were 82.23% 92.31% at 4 levels, and the relative standard deviations were 2.13% 4.76% (n=6). The method has excellent sensitivity and stability, and meets the requirements for the analysis and detection of phenolic compounds such as 2-tert-butylphenol, 4-tert-butylphenol and 2,4-di-tert-butylphenol in polycarbonate plastic packaging materials. Accurate quantification.